3Flex

Accessories

Specifications

3Flex Physisorption Only

3Flex Chemisorption

Chiller Dewar Liquid Recirculation System

Analysis

Analysis Range 1.3 x 10 -9 to 1.0 P/P 0

1 x 10 -6 to 900 torr

Micromeritics’ Chiller Dewar is a closed loop recirculating system that utilizes a high surface area copper coil to provide excellent heat transfer between the dewar and the recirculating liquids. Temperature control is provided through an external recirculating bath or chiller bath which are supplied as accessory items.

up to 3, one port dual purpose chemisorption and physisorption

Available Micropore Ports up to 3

Dosing and Evacuation Control Proprietary Servo

Proprietary Servo 4 stage diaphragm Standard 2 or 3 ports

Roughing Pump 4 stage diaphragm

Krypton Analysis Standard 1 port, optional up to 3 ports

Temperature Range

-50 °C to 200 °C

Analysis Gas Per Sample Ability to use up to 3 gases concurrently, one probe gas on each port Minimum Measurable Surface Area Standard 0.01 m 2 /g

Temperature Stability

±0.01 °C

ISO Controller Sub-Ambient, Thermoelectric Cooled Dewar

0.01 m 2 /g

Krypton 0.0005 m 2 /g

0.0005 m 2 /g

Micromeritics’ ISO Controller utilizes thermoelectric cooling based on the Peltier principle. The unit is designed to maintain a constant temperature between -5 °C and 80 °C when using CO 2 , N 2 , and other gases for adsorption analysis. The device rapidly cools and efficiently maintains temperature with minimal electrical current required.

Instrument Control and Features

Temperature Control 45 °C, ±0.05 °C with 3 strategically placed RTDs 45 °C, ±0.05 °C with 3 strategically placed RTDs Adsorptive Gas Inlets 6 12 standard; optional up to 16 Vapor Sorption Option Standard ports 1 and 2, optional heated Standard ports 1 and 2, optional heated

Programmable- 0.1–50 °C/minute 50 °C/min to 600 °C 20 °C/min from 600 to 800 °C 10 °C/min from 800 to 1100 °C

The dewar section is placed on the instrument dewar elevator and then raised into position for analysis.

Furnace (chemisorption model only)

N/A

Mass Flow Controller (chemisorption model only) TCD w/cold trap (chemisorption model only)

Temperature Range

-5 °C to 80 °C (lab temp <27 °C)

N/A

Standard, flow up to 200 cm 3 /m, ±1% of set point

Cooling Capacity

Approx. 80W at 0 °C, 120W at 25 °C

N/A

Optional two levels of available performance

Minimum Controllable Resolution

0.1 °C

Heated port for connection of external detectors including an available Cirrus ™ Quadrapole Mass Spec 3 in situ, 6 additional with SmartVac Prep

Standard External Dedicated Port N/A

Temperature Stability

±0.1 °C

Degas 3 in situ, 6 additional with SmartVac Prep

A/D data acquisition 29 bit (effective 25)

29 bit (effective 25)

Cryostat I Single-Stage Cryogenic Refrigerator Based on the Gifford-McMahon Principle

Pressure Transducer System up to 12

up to 12

1000 torr 0.12% reading 10 torr 0.12% reading 0.1 torr 0.15% reading

1000 torr 0.12% reading 10 torr 0.12% reading 0.1 torr 0.15% reading

Transducer Accuracy

The Micromeritics Cryostat I is a closed-cycle cryocooler based on the Gifford-McMahon (GM) refrigeration principle. It uses helium gas from a helium compressor to generate cryogenic temperatures.

Cryogen

Cryogen Dewar 3.2 L, greater than 70 hrs virtually unlimited with refill during analysis

3.2 L, greater than 70 hrs virtually unlimited with refill during analysis

The Cryostat I eliminates the need for liquid nitrogen and can obtain temperatures below the 77 K of liquid nitrogen.

Cryogen Free Space Control Isothermal Jacket

Isothermal Jacket

Reports

Advanced Modeling GAB, Sips, Toth, dissociative Langmuir, Redlich-Peterson Instrument Operation Dashboard Dashboard permits real-time monitoring of critical parameters Minimized Bench Space Footprint Height 112 cm 112 cm Width 57.2 cm 57.2 cm Depth 61 cm 61 cm

Temperature Range

25 to 350 K

400

LiquidNitrogenDewar Cryostat

350

Temperature Stability

±0.005 K

QuantityAdsorbed (cm 3 /gSTP) 0.0 50 100 150 200 250 300 0.1

Desorption Isotherm

Nitrogen Reservoir

closed-cycle helium

Adsorption Isotherm

Cool Down Time to Stated Minimum from Ambient

60 minutes

0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9

RelativePressure (p/p o )

Provided specifications were valid as taken from available documents at time of publication. These specifications may change without notice and are only provided as a general reference.